CHEMICAL ENGINEERING CENTRAL RESEARCH LABORATORY (KİMAL)

chemIcal engIneerIng departmant

 

EQUIPMENTS in KİMAL

 

 a) Pure and Applied Science’s Research Equipments:

 

1. Atomic Absorption Spectrophotometer (AAS); GBC A4382.

2. Flame Photometer; Jenway PFR-7.

3. Gas Chromatography (GC); Shimadzu GC-14B.

4. Gas Chromatography-Mass Spectrometer (GC-MS); Shimadzu GC-17A/GC-MS-QP-5000.

5. High Performance Liquid Chromatography (GPC-HPLC); Shimadzu LC-10A.

6. Fourier Transformer Infrared Spectrophotometer (FTIR); Shimadzu 8300.

7. Ultraviolet-Visible Region Spectrophotometer (UV-VIS); Shimadzu UV-1601.

8. Ultraviolet-Visible Region Spectrophotometer (UV-VIS); Shimadzu UV-2401.

9. Thermogravimeter (TGA); Shimadzu DT-50.

10. Differential Thermal Analysis (DTA); Shimadzu DT-50.

11. Differential Scanning Calorimeter (DSC); Shimadzu DT-50.

12. Binocular Microscope.

Except Flame Photometer all Equipments connected a Computer.

 

 b) Engineering Research Equipments:

 

1. Full Automatic Flow Index Test Equipment; Ceast 6941

2. Universal Test Equipment; Hounsfield H5K-S

3. Digital Hardness Equipment; Digiroc RB

4. Solid-Liquid Extraction System; Velp SER-148

5. Supercritical Fluid Extraction Equipment (SFE); Isco, SFX 220

6. Chimney Smoke Analysis Equipment; Testo 350

7. Flash Point Equipment; ISL FP9356

8. Crossflow Ultrafiltration System; Sartorius Trademark

9. Process Control System with Advantech VisiDAQ software

Except Chimney Smoke Analysis and Hardness Equipments the others connected a Computer

 

c) Polymer Technology Equipments:

 

1. Plastic Injection Machine; Coşhan KLB-250GR.

2. Plastic Breaking Machine; Coşhan CMS-4027.

3. PE Blowing up Machine; Yelken Q 60.

 

 

THE ANALYSIS DONE BY THE EQUIPMENTS IN KIMAL

 

Gas Chromatography - Mass Spectrophotometer (GCMS)

*The equipment has a “Quadropole” system.

*The equipment works with EI (Electron Impact) and CI (Chemical Ionization) methods.

*The equipment has “NIST 62” and “Pesticide” libraries.

 

Qualitative and quantitative analysis of

* Petrochemicals, food, pharmaceutics and biochemical products, organic and inorganic compounds

*Volatile oil, fat acids of plant extracts

*Petroleum (saturated and unsaturated hydrocarbons, naphthalene and its derivatives, phenols, etc.)

*Medical analysis (medicine, narcotics and metabolites).

 

Gas Chromatography (GC)

*Equipment has FID (Flame Ionization Detector) and ECD (Electron Coupled Detector) systems.

*The equipment has TC-WAX, TC-1, TC-5 columns.

 

* Quantitative analysis of volatile petrochemicals, food, pharmaceutics and biochemical products, organic and inorganic compounds

* Volatile oil analysis of plant extracts

*Pesticide analysis

*Phenol analysis

*Alcohol analyses, etc.

 

High Performance Liquid Chromatography (HPLC)

*The equipment has  Refractive Index” and “UV-VIS” detector systems.

*The equipment has two chromatographic pumps.

*System is suitable for double gradient, high pressure, low pressure experiments.

*The equipment has various LC and GPC columns.

 

*Pharmaceutics (antibiotics, sedatives, steroids, analgesics),

*Biochemistry (amino acids, proteins, carbohydrates, lipids) ,

*Food products (artificial flavor, antioxygen, aflatoxins, additive materials),

*Industrial chemicals (condensed aromatics, surfactants, paints),

*Indistinct (pesticides, herbicides, phenols, PCB’s),

*Judicial medicine (medicine, poisons, alcohol at blood, narcotics),

*Clinical medical (ballast acids, medical metabolites, urine extracts).

 

Atomic Absorption Spectrophotometer (AAS)

*Working method based on atomic absorption and emission.

*The system has 190-900 nm wavelength ground correction.

*Equipment has both flame and graphite atomizer.

*Analysis of Ca, Mg, Co, Cr, Cu, Fe, Mn, Ni, As and Hg elements at petrochemicals, food, pharmaceutics and biochemical products

* Mineral analysis

*Analysis of  (Ca, Mg, Cu, Fe, Mn, Hg) in fruit juice,  (Cu, Fe) in wine and animal fodder

* Analysis of Cu at Biological materials, blood, urine and tissue samples, Fe at urine, Ca, Mg, Cu, Mn at bone tissue

* Analysis of Ca, Mg, Cu  in sea water,

* Fe analysis at tap water,

* Mg analysis at organometalic compounds

UV-Visible Region Spectrophotometer

*Equipment has  double light way.

*There is “static temperature control system” at 1601 model.

*Sensitive limit is approximately 10–4–10-5 M

 

* Qualitative and quantitative analysis of inorganic and organic compounds (between 190-1600 nm wavelengths),

*Surface chemistry and kinetic studies,

* Complex material structure determinations

*Functional group determinations.

 

Fourier Transformer Infrared Spectrophotometer (FTIR)

*Equipment works between 4000-650 cm–1 wave numbers.

*Equipment has a library.

*Qualitative and quantitative analysis of liquid and solid compounds

* Qualitative and half quantitative analysis of a lot of materials in agriculture and industry

* Structure determination and kinetic studies of inorganic and organic materials

Supercritical Fluid Extraction System (SFE)

 

 

Supercritical CO2 extraction of natural plant materials such as antioxidants seed oils, vitamins, pharmaceutical compounds etc

.

 

 

 

 

Thermal Analysis Units

Thermogravimeter (TGA)

Differential Thermal Analysis (DTA)

Differential Scanning Calorimeter (DSC)

Thermal analysis of,

*Minerals, such as silicates, clays, ferrite, ceramic, glass, etc.

*Inorganic materials, catalysts

*Metals and alloys, polymers, medicine

Determination of,

*Glass transition, melting and boiling points and heats of organic compounds

 

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